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Examination of metals and alloys

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Metallurgical examination of metals (alloys) is carried out in order to detect metal particles and traces of metallization at objects, to study the qualitative and quantitative composition of metals and alloys and products from them, to establish the technology and time for the manufacture of products from metals and alloys, their operating conditions, modifications associated with circumstances of the event.

The objects of metallurgical expertise are very diverse:

  • steel products and their blanks: home-made and factory-made knives, daggers, daggers, brass knuckles and other steel objects serving as instruments of crime, their fragments, debris;
  • fragments and details of explosive devices, shells, mines;
  • parts of destroyed parts of vehicles and other mechanisms;
  • particles and sawdust of locking and signaling devices;
  • wire;
  • cable products, metal pipes, metal hoses and their fragments;
  • articles made of precious metals and alloys, jewelry, native gold;
  • traces of metallization;
  • products and parts thereof made of non-ferrous metals for household use (dishes, garments, etc.) and much more.

Details ...

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Objects of metallurgical expertise are seized in almost all categories of criminal and civil cases and can be objects of research not only for this kind of expertise, but also for complex metallurgical, other classes and types of expertise: trasological, electrical, fire-technical, ballistic, explosive, autotechnical. Metallurgical expertise is in demand by the customs authorities for foreign trade operations. / P>

The most common diagnostic questions are:

  • what metal, alloy this item is made of (fragment);
  • what is the brand of this metal, alloy; what is the scope of this metal, alloy;
  • whether there is a metal coating on the presented object;
  • what are its composition and purpose; whether there are metal particles on the carrier object; what is their composition; for the manufacture of what household products this metal could be intended;
  • whether there are traces of metallization on the carrier object and what composition; what is the source of their origin; the object of what shape and size they could be left;
  • whether the metal (alloy) presented for research is precious; what is the percentage of components in it and what sample does it correspond to; whether this gold is native or industrial; whether this piece of jewelry is made of native or industrial gold; from which deposit this native gold originates;
  • what is the method of manufacturing this product; what processing it was subjected to; how long the object was oxidized (rusty); what are the causes and mechanism of destruction of this metal object (node, part);
  • whether a metal coin or medal is counterfeit; what alloy of them and in what way (for example, casting into a non-metallic or metallic form, stamping using a matrix and a punch made by engraving, etc.) it was made;
  • whether there are traces of melting on the presented metal objects; whether the melting of cable products (electrical wires and cables), metal pipes and metal hoses, electrical panel housings and other products occurred as a result of external thermal effects or emergency operation of the power grid; if reflow occurred due to emergency mode, then under what conditions (for example, before the fire: room temperature and the absence of combustion products in the air, or during the development of a fire: in conditions of high temperature and smoke);
  • how is this metal object divided into parts; whether a thermal cutting device was used for this, the type of this device; what welding consumables were used for cutting; what was the qualification of the person who performed the electric arc (oxy-fuel) cutting.

Identification issues within the framework of the metallurgical expertise include:

  • whether the metal or alloy from which the products and comparative samples are made (for example, a ring and an ingot of gold) have a common group affiliation in composition;
  • whether a metal product (fragment) and comparative samples have a common group affiliation in terms of manufacturing and operation features;
  • whether this object and comparative samples were made from the same alloy, steel grade;
  • whether this metal fragment is part of this product (a metal particle removed from the victim's body and a knife, a plate with a number and a car body, etc.);
  • whether this object is made from a specific metal object (a knife blade from a given steel plate, a crown from discovered industrial gold);
  • whether the compared metal objects belong to a single source of origin: to the products of one plant (for example, sheets of roofing iron), a single batch, a single mass (native gold and gold particles on a microbalance);
  • at the same or different deposits, gold was mined, seized from several suspects (or is this native gold mined at a certain deposit, is this jewelry made of gold from a certain deposit).

Microparticles of metals and alloys and traces of metallization (in combination with other objects) can be used to establish the fact of contact interaction of objects.

For example, when conducting a metallurgical examination of fused wires, the metallurgical examination establishes the conditions for the formation of metal fusion; in combination with the electrical one - issues related to the causes of emergency operation of the power grid are resolved, and in combination with the fire-technical one - the presence of a cause-and-effect relationship in the emergency mode in the power grid, conductor melting and fire

As part of the metallurgical expertise, small permanent magnets are used to detect microparticles of ferrous metals. Microparticles of metals and alloys and traces of metallization are removed together with the carrier object. Fragments of electrical wiring containing reflow are marked, the places of their removal are indicated on the electrical diagram of the object and its plan.

To carry out a metallurgical examination, metal objects are each packed separately in paper bags or cardboard boxes and supplied with explanatory notes. If there are foreign deposits on them, for example, blood, or objects are damp (the knife is removed from the reservoir), they must be dried at room temperature before packing. Sealed packaging of wet metal objects or objects with biological layers, for example, in plastic wrap, is highly undesirable, since metal corrosion and decomposition (decay) of layers may begin.

Examination of metals and alloys

Service (for 1 sample) Deadlines Price without VAT*
X-ray fluorescence analysis
X-ray fluorescence spectrometry (XRF) up to 4 days 44 USD
X-ray fluorescence spectrometry (XRF, without issuing a protocol) up to 2 days 23 USD
Sample preparation for XRF mechanical up to 3 days 44 USD
Sample preparation for XRF with annealing (2 samples) up to 7 days 81 USD
Determination of alloy grade (alloying + carbon + grade) up to 7 days 102 USD
Determination of alloy grade (alloying + carbon + grade, without issuing a protocol) up to 4 days 84 USD
Determination of the carbon content (AN-7529, 0.03-99.99) up to 7 days 93 USD
Atomic emission analysis
Inductively Coupled Plasma Atomic Emission Spectrometry (ICPE, >5 ppm, per sample) up to 14 days 105 USD
Qualitative analysis of all elements (ICPE, screening, >5 ppm) up to 14 days 105 USD
Quantitative analysis of one element (ICPE, >1-10 ppb, for 1 element) up to 14 days 140 USD
Sample preparation for ICPE up to 14 days 40 USD
Analytical chemistry
Methods of analytical chemistry, simple method up to 7 days 130 USD
Methods of analytical chemistry, complex technique up to 14 days 267 USD
X-ray diffraction
Powder X-ray diffraction (XRD) up to 14 days 151 USD
Sample preparation of solid or liquid samples for XRD up to 3 days 44 USD
Coating expertise
Coating thickness determination (ISO 2808):
magnetic induction method (10 points, 3-5000 microns) up to 5 days 56 USD
eddy current method (per 1 sample, 10 points, 5-2000 µm) up to 5 days 51 USD
metric method (5 points, 10-2500 microns) up to 3 days 47 USD
drip method (5 points, from 2.5 µm) up to 5 days 74 USD
XRF method (ISO 3497, 1 point, from 0.01 µm) up to 4 days 44 USD
gravimetric method (arbitration, 3 points, no limit) up to 7 days 144 USD
Sample preparation (removal of coating, up to 10 points) up to 7 days 28 USD
Thickness measurement
Thickness by ultrasonic method (per 1 sample, 5 points, 0.8-300 mm) up to 7 days 56 USD
Thickness by metric method (per 1 sample, 5 points, 0.01-25.0 mm) up to 7 days 47 USD
Measurement of roughness
Surface roughness (per 1 sample, 2-300 µm) up to 7 days 49 USD
Surface roughness (per 1 sample, Ra 0.005-16 µm, Rz 0.02-160 µm) up to 14 days 460 USD
Metal hardness measurement
Hardness on a stationary device (HB, HRC, HRB, HV) (per 1 sample) up to 14 days 86 USD
Hardness on a portable device (ASTM A956) up to 7 days 63 USD
Microhardness (per 1 sample, 5 injections) up to 14 days 95 USD
Preparation of standard samples for mechanical testing up to 7 days 123 USD
Mechanical testing of metal and alloys
Mechanical test for abrasion (first hour) up to 7 days 37 USD
Mechanical test for abrasion (every subsequent hour) up to 1 day 5 USD
Mechanical tensile testing of samples (2-5 samples, до 200 kН) up to 14 days 160 USD
Mechanical testing of samples for bending (2-5 samples) up to 14 days 160 USD
Mechanical tests of samples for compression (2-5 samples) up to 14 days 160 USD
Impact test at room temperature (2-5 samples) up to 14 days 133 USD
Impact testing at low temperatures (from 0 to -80 °С, 2-5 samples) up to 14 days 153 USD
Preparation of standard samples for mechanical testing up to 14 days 153 USD
Metallographic studies and SEM
Metallographic study of the structure (preparation, etching, grain, structure) up to 14 days 251 USD
Electron micrograph + quantitative analysis of the composition (SEM EP-XRF, up to 5 points) up to 14 days 156 USD
Sample preparation for microphotography (cutting, polishing, grinding, drying, vacuuming, deposition) up to 14 days 70 USD
Flaw detection of metals and alloys
Capillary control (first dm2) up to 7 days 74 USD
Capillary control (each subsequent dm2) up to 7 days 16 USD
Magnetic particle inspection (MPD, first dm2) up to 7 days 100 USD
Magnetic particle inspection (MPD, each subsequent dm2) up to 7 days 33 USD
Visual-optical control of joints (first line) up to 7 days 49 USD
Visual-optical control of joints (each subsequent l.m.) up to 7 days 19 USD
Visual-optical control of the base metal (first m2) up to 7 days 49 USD
Visual-optical control of the base metal (each subsequent m2) up to 7 days 19 USD
Ultrasonic flaw detection of joints (first line) up to 7 days 67 USD
Ultrasonic flaw detection of joints (each subsequent r.m.) up to 7 days 19 USD
Base metal ultrasonic testing (first m2) up to 7 days 67 USD
Ultrasonic flaw detection of the base metal (each subsequent m2) up to 7 days 21 USD
Determining the causes of damage and breakdowns
Fractographic analysis of fractures (for 1 fracture) up to 14 days 226 USD
Determining the causes of damage (for 1 question) up to 14 days 226 USD
Study of bank bullion
Inspection of the metal surface for compliance with the sample (XRF) up to 4 days 44 USD
Checking the homogeneity of the metal (ultrasound) up to 7 days 56 USD
Checking the density of metal (hydrostatics) up to 3 days 47 USD
other services
Compliance with certificates and other documents, confirmation or refutation of brand conformity (without the cost of brand identification) up to 14 days 35 USD
Radioactivity level (gamma and beta background) up to 3 days 35 USD

The prices are approved by the director of LLC "In Consulting" 02.11.2024. Deadlines are indicated in working days

For a free consultation, you can use On-line consultation, or call us or write to the messengers.For information about the cost of services go to Tariffs or place Application for Services.